Ceramic Industry News

Study Finds More than Half of Labs' Results Inaccurate

According to a new report by the Toxics in Packaging Clearinghouse (TPCH), 16% of laboratory test results for lead and cadmium in packaging samples were “unacceptable.” The TPCH sent packaging samples to six private analytical laboratories and the California Department of Toxic Substances Control Environmental Chemistry Laboratory. The samples were used to assess performance in testing for toxic metals in packaging. Specifically, the study assessed the performance of laboratories in measuring the total concentrations of four metals: lead, cadmium, mercury and chromium. The use of lead, cadmium, mercury and hexavalent chromium is restricted in packaging by law in 19 U.S. states.

Over half the laboratories (four of seven) reported one or more unacceptable results. A result was considered unacceptable if it varied by more than 25% from the average of all laboratories’ results, as well as from an X-ray fluorescent (XRF) analysis.

“The good news is that only one packaging sample of the 42 analyzed (< 2%) by the seven labs resulted in a false negative,” said Alex Stone, Ph.D., a chemist with the Department of Ecology in Washington State. “A false negative is a test result indicating the sample is in compliance with state laws when it isn’t. Such results could lead a company to believe they are in compliance with our state laws when they are not.”

Overall, the quality and consistency in laboratory testing results was reportedly better than the TPCH expected, given past experiences with laboratory test data. For the last five years, the TPCH has screened packaging for compliance with state toxics in packaging laws using XRF analysis. XRF analysis is a rapid and inexpensive screening tool for measuring the elemental composition of samples, including the four metals regulated by state laws. The TPCH expected XRF screening results of packaging samples to have some level of correlation with laboratory analysis, and was surprised this was not often the case.

“We believe that the discrepancy between XRF and laboratory analysis can be traced to the selection of sample preparation methodologies,” said Ron Ohta, California Department of Toxic Substances Control, which funded the TPCH study. “Measuring the total concentration of metals requires that the sample be completely dissolved. We don’t believe that some labs are paying careful enough attention to this critical performance goal, resulting in analytical results that underreport the amount of heavy metals, particularly cadmium and lead, used in packaging.”

The TPCH report emphasizes the importance of communicating to laboratories test requirements and data quality objectives. Specifically, total concentration of the restricted metals is possible only through complete sample decomposition. If total sample decomposition is not achieved, the laboratory should state so on the test report, as it strongly impacts the accuracy of the results.

For more information, visit www.toxicsinpackaging.org.

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